TABLE 1. List of the Khok Sung vertebrate fauna [after Claude et al. (2011), Martin et al. (2012), Suraprasit et al. (2015, 2016)].
Mammalia | ||
Proboscidea | ||
Stegodontidae | ||
Stegodon cf. orientalis | ||
Elephantidae | ||
Elephas sp. | ||
Perissodactyla | ||
Rhinocerotidae | ||
Rhinoceros sondaicus | ||
Rhinoceros unicornis | ||
Artiodactyla | ||
Bovidae | ||
Bos sauveli | ||
Bos gaurus | ||
Bubalus arnee | ||
Capricornis sumatraensis | ||
Cervidae | ||
Axis axis | ||
Rucervus eldii | ||
Rusa unicolor | ||
Suidae | ||
Sus barbatus | ||
Primates | ||
Cercopithecidae | ||
Macaca sp. | ||
Carnivora | ||
Hyaenidae | ||
Crocuta crocuta ultima | ||
Canidae | ||
Cuon sp. | ||
Reptilia | ||
Testudines | ||
Geoemydidae | ||
Batagur cf. trivittata | ||
Heosemys annandalii | ||
Heosemys cf. grandis | ||
Malayemys sp. | ||
Trionychidae | ||
Chitra sp. | ||
cf. Amyda sp. | ||
Crocodilia | ||
Gavialidae | ||
Gavialis cf. bengawanicus | ||
Crocodylidae | ||
Crocodylus cf. siamensis | ||
Squamata | ||
Varanidae | ||
Varanus sp. | ||
Boidae | ||
Python sp. | ||
Actinopterygii | ||
Siluridae indet. | ||
Aves | ||
Galliformes indet. |
TABLE 2. Details of the five fossil teeth collected from unit F for ESR dating purpose.
Lab code | Collection number | Description |
3545 | DMR-KS-05-03-00-107 | Molar fragment of Stegodon cf. orientalis |
3546 | DMR-KS-05-03-28-13 | Left M3 of Bubalus arnee |
3547 | DMR-KS-05-03-31-5 | Right M1 of Bubalus arnee |
3548 | DMR-KS-05-04-01-7 | Right P3 fragment of Bos sauveli |
3549 | DMR-KS-05-03-23-2 | Left M1 or M2 of Bos sauveli |
TABLE 3. ESR results derived from the dating analyses of the six tooth samples. Note that samples 3546A and 3546B belong to the same tooth. Measurement precision is expressed as the mean coefficient of variation of the ESR intensities derived from all the aliquots of a given sample after the three repeated measurements. De precision is the variability of the De values derived from the repeated measurements of a given sample. The final De error is a combination of the fitting error (see Figure 4) and the error on the calibration of the irradiation source (2.3%).
Sample | Measurement precision (%) |
DE precision (%) |
Adj. r-Square | DE value (Gy) |
Dmax/DE |
3545 | 1.0 | 0.8 | 0.9972 | 73.2 ± 4.2 | 8.8 |
3546A | 0.8 | 2.0 | 0.9988 | 99.4 ± 4.3 | 6.5 |
3546B | 0.9 | 0.5 | 0.9990 | 131.5 ± 5.1 | 7.6 |
3547 | 0.9 | 0.7 | 0.9983 | 135.7 ± 6.3 | 7.4 |
3548 | 0.5 | 0.3 | 0.9983 | 313.0 ± 13.1 | 6.4 |
3549 | 0.9 | 0.6 | 0.9988 | 124.0 ± 4.9 | 8.1 |
TABLE 4. Radioelement concentrations obtained from the ICP-MS analyses of several samples taken from the raw sediment of unit F and from the crust attached to the fossil bones. Minimum, maximum and mean values and associated one standard error are displayed. The corresponding coefficients of variation are displayed in parenthesis.
Sample ID | Associated fossil remain | U (ppm) | Th (ppm) | K (ppm) |
Sediment samples | ||||
#s1 | Turtle plate | 1.18 ± 0.08 | 2.79 ± 0.13 | 0.25 ± 0.01 |
#s2 | Gavialis plate | 7.98 ± 0.29 | 1.99 ± 0.10 | 0.31 ± 0.01 |
#s3 | Stegodon foot bone | 8.28 ± 0.30 | 2.74 ± 0.12 | 0.30 ± 0.01 |
#s4 | Stegodon cf. orientalis vertebra | 2.49 ± 0.11 | 2.37 ± 0.11 | 0.40 ± 0.02 |
#s5 | Stegodon cf. orientalis vertebra | 1.78 ± 0.09 | 2.45 ± 0.11 | 0.37 ± 0.01 |
#s6 | Bubalus arnee horn core | 8.69 ± 0.31 | 5.66 ± 0.24 | 0.58 ± 0.02 |
#s7 | Bubalus arnee vertebra | 0.96 ± 0.08 | 2.48 ± 0.11 | 0.26 ± 0.01 |
#s8 | Large bovid long bone | 1.44 ± 0.09 | 3.71 ± 0.16 | 0.43 ± 0.02 |
#s9 | Rhinoceros unicornis calcaneus | 3.05 ± 0.13 | 1.75 ± 0.09 | 0.45 ± 0.02 |
#s10 | Mandible of cervid | 2.47 ± 0.11 | 2.71 ± 0.12 | 0.27 ± 0.01 |
#s11 | Skull of Bubalus arnee | 2.75 ± 0.12 | 3.06 ± 0.14 | 0.46 ± 0.02 |
#s12 | Skull of Bubalus arnee | 2.87 ± 0.12 | 2.73 ± 0.12 | 0.36 ± 0.01 |
#s13 | Large bovid vertebra | 12.48 ± 0.44 | 3.31 ± 0.15 | 0.41 ± 0.02 |
Range | 0.96-8.69 | 1.75-5.66 | 0.25-0.58 | |
Mean and standard error | 4.34 ± 1.02 (23.6%) |
2.90 ± 0.27 (9.3%) |
0.37 ± 0.03 (7.1%) |
|
Sample ID | Associated fossil remain (sediment sample) | U (ppm) | Th (ppm) | K (ppm) |
Crust samples | ||||
#c1 | Stegodon cf. orientalis vertebra (#s4) | 0.58 ± 0.07 | 2.09 ± 0.10 | 0.34 ± 0.01 |
#c2 | Stegodon cf. orientalis vertebra (#s4) | 0.55 ± 0.07 | 2.21 ± 0.10 | 0.33 ± 0.01 |
#c3 | Stegodon cf. orientalis vertebra (#s5) | 1.92 ± 0.10 | 7.79 ± 0.33 | 0.63 ± 0.02 |
#c4 | Large bovid long bone (#s8) | 0.78 ± 0.07 | 1.68 ± 0.09 | 0.37 ± 0.01 |
Range | 0.55-1.92 | 1.68-7.79 | 0.33-0.63 | |
Mean and standard error | 1.02 ± 0.32 (32.0%) |
4.03 ± 1.45 (36.1%) |
0.43 ± 0.07 (16.4%) |
TABLE 5. Data inputs for the combined US-ESR age calculations. Note that samples 3546A and 3546B belong to the same tooth. Apparent U-series ages with 2-σ errors are also provided in italics. Key: n/a = not applicable; (1) after Grün and Katzenberger-Apel (1994); (2) A 10% error was assumed; (3) assumed value (note the impact of this parameter is minimum: by considering removed thicknesses of between 20 and 60 µm, the resulting age varies by <1%); (4) used for beta dose rate evaluation only: these values correspond to 75% of the mean concentrations obtained from the crust samples and 25% of the mean concentrations derived from the sediment samples. All errors are given at a 1-σ confidence level.
SAMPLE | 3545 | 3546A | 3546B | 3547 | 3548 | 3549 |
Enamel | ||||||
Dose (Gy) | 73.2 ± 4.2 | 99.4 ± 4.3 | 131.5 ± 5.1 | 135.7 ± 6.3 | 313 ± 13.1 | 124.0 ± 4.9 |
U (ppm) | 0.414 ± 0.084 | 0.109 ± 0.035 | 0.109 ± 0.035 | 0.158 ± 0.049 | 0.508 ± 0.074 | 0.391 ± 0.580 |
234 U/ 238 U | 1.802 ± 0.008 | 1.799 ± 0.011 | 1.799 ± 0.011 | 1.722 ± 0.012 | 1.581 ± 0.010 | 1.837 ± 0.014 |
230 Th/ 234 U | 0.480 ± 0.004 | 0.352 ± 0.006 | 0.352 ± 0.006 | 0.399 ± 0.050 | 0.500 ± 0.014 | 0.356 ± 0.009 |
Apparent U-series age (ka) | 67.5 ± 1.6 | 45 ± 7 | 45 ± 7 | 53.5 ± 1.7 | 72.0 ± 5.4 | 46.3 ± 0.9 |
Alpha Efficiency (1) | 0.13 ± 0.02 | 0.13 ± 0.02 | 0.13 ± 0.02 | 0.13 ± 0.02 | 0.13 ± 0.02 | 0.13 ± 0.02 |
Water content (%) | 0 | 0 | 0 | 0 | 0 | 0 |
Initial enamel thickness (μm) (2) | 4600 ± 800 | 1360 ± 160 | 1360 ± 160 | 960 ± 270 | 1100 ± 220 | 960 ± 70 |
Tissue 1 (dentine) | ||||||
U (ppm) | 66.6 ± 5.9 | 1.88 ± 0.07 | 1.88 ± 0.07 | 37.7 ± 8.1 | 169.2 ± 8.7 | 67.1 ± 5.3 |
234 U/238 U | 1.811 ± 0.003 | 1.735 ± 0.006 | 1.735 ± 0.006 | 1.691 ± 0.001 | 1.624 ± 0.001 | 1.852 ± 0.001 |
230 Th/234 U | 0.133 ± 0.001 | 0.128 ± 0.002 | 0.128 ± 0.002 | 0.122 ± 0.001 | 0.526 ± 0.001 | 0.12 ± 0.001 |
Apparent U-series age (ka) | 15.4 ± 0.1 | 14.7 ± 0.6 | 14.7 ± 0.6 | 14.1 ± 0.1 | 76.9 ± 0.4 | 13.8 ± 0.1 |
Water (%) | 20 ± 10 | 20 ± 10 | 20 ± 10 | 20 ± 10 | 20 ± 10 | 20 ± 10 |
Removed enamel thickness (μm)(2, 3) | 100 ± 30 | 30 ± 10 | 30 ± 10 | 30 ± 10 | 30 ± 10 | 30 ± 10 |
Tissue 2 | ||||||
U (ppm) | n/a | n/a | 158.1 ± 8.9 | n/a | n/a | n/a |
234 U/238 U | n/a | n/a | 1.774 ± 0.001 | n/a | n/a | n/a |
230 Th/234 U | n/a | n/a | 0.237 ± 0.001 | n/a | n/a | n/a |
Apparent U-series age (ka) | n/a | n/a | 28.9 ± 0.1 | n/a | n/a | n/a |
Water (%) | n/a | n/a | 20 ± 10 | n/a | n/a | n/a |
Removed enamel thickness (μm)(2, 3) | n/a | n/a | 30 ± 10 | n/a | n/a | n/a |
Sediment | ||||||
U (ppm)(4) | 2.64 ± 0.17 | 2.64 ± 0.17 | 2.64 ± 0.17 | 2.64 ± 0.17 | 2.64 ± 0.17 | 2.64 ± 0.17 |
Th (ppm) (4) | 2.80 ± 0.09 | 2.80 ± 0.09 | 2.80 ± 0.09 | 2.80 ± 0.09 | 2.80 ± 0.09 | 2.80 ± 0.09 |
K (%) (4) | 0.34 ± 0.07 | 0.34 ± 0.07 | 0.34 ± 0.07 | 0.34 ± 0.07 | 0.34 ± 0.07 | 0.34 ± 0.07 |
Water (%) | 30 ± 10 | 30 ± 10 | 30 ± 10 | 30 ± 10 | 30 ± 10 | 30 ± 10 |
Removed thickness (μm)(2, 3) | 30 ± 10 | 30 ± 10 | - | 30 ± 10 | 30 ± 10 | 30 ± 10 |
Depth (m) | 5 ± 1 | 5 ± 1 | 5 ± 1 | 5 ± 1 | 5 ± 1 | 5 ± 1 |
TABLE 6. Data outputs from the combined US-ESR age calculations. Note that samples 3546A and 3546B belong to the same tooth. Scenario A corresponds to the use of a gamma dose rate of 658 ± 160 µGy/a, while scenario B is based on 342 ± 63 µGy/a instead. Key: p-enamel, p-tissue1 (dentine) and p-tissue2 correspond to the uptake parameter values calculated for each dental tissue as in Grün et al. (1988). Post-Rn equilibrium was assumed in dental tissues and sediment. All errors are given at a 1σ confidence level.
SAMPLE | 3545 | 3546A | 3546B | 3547 | 3548 | 3549 |
Scenario A | ||||||
Internal dose rate (μGy/a) | - | 14 ± 6 | 14 ± 6 | 21 ± 9 | 90 ± 53 | 54 ± 16 |
Beta dose rate, tissue 1 (dentine) (μGy/a) | - | 4 ± 0 | 3 ± 0 | 118 ± 40 | 999 ± 393 | 175 ± 41 |
Beta dose rate, sediment or tissue 2 (μGy/a) | 13 ± 3 | 44 ± 9 | 295 ± 91 | 61 ± 17 | 54 ± 13 | 61 ± 12 |
Gamma dose rate (μGy/a) | 658 ± 160 | 658 ± 160 | 658 ± 160 | 658 ± 160 | 658 ± 160 | 658 ± 160 |
Cosmic dose rate (μGy/a) | 109 ± 12 | 109 ± 12 | 109 ± 12 | 109 ± 12 | 109 ± 12 | 109 ± 12 |
Total dose rate (μGy/a) | - | 830 ± 160 | 1069 ± 184 | 968 ± 166 | 1911 ± 427 | 1058 ± 166 |
p-enamel | - | 0.35 | 0.41 | 0.31 | -0.03 | 0.27 |
p-tissue 1 (dentine) | - | 0.98 | 1.99 | 0.00 | -0.16 | 1.61 |
p-tissue 2 | - | - | 1.87 | - | - | - |
Combined US-ESR age (ka) | age calculation impossible | 119 + 36 -20 | 123 + 30 -21 | 140 + 35 -21 | 163 + 47 -29 | 117 + 25 -16 |
Combined CSUS-ESR age (ka) | 79 ± 16 | 120 ± 24 | 133 ± 28 | 156 ± 31 | 216 ± 45 | 135 ± 26 |
Scenario B | ||||||
Internal dose rate (μGy/a) | 96 ± 31 | 10 ± 4 | 9 ± 4 | 15 ± 6 | 71 ± 43 | 37 ± 10 |
Beta dose rate, dentine (μGy/a) | 40 ± 11 | 3 ± 0 | 1 ± 0 | 79 ± 27 | 794 ± 332 | 121 ± 24 |
Beta dose rate, sediment or cement (μGy/a) | 13 ± 3 | 44 ± 9 | 179 ± 53 | 61 ± 17 | 54 ± 13 | 61 ± 12 |
Gamma dose rate (μGy/a) | 342 ± 63 | 342 ± 63 | 342 ± 63 | 342 ± 63 | 342 ± 63 | 342 ± 63 |
Cosmic dose rate (μGy/a) | 109 ± 12 | 109 ± 12 | 109 ± 12 | 109 ± 12 | 109 ± 12 | 109 ± 12 |
Total dose rate (μGy/a) | 601 ± 72 | 509 ± 64 | 638 ± 83 | 607 ± 71 | 1371 ± 341 | 671 ± 70 |
p-enamel | -0.37 | 1.66 | 1.84 | 1.50 | 0.59 | 1.43 |
p-tissue 1 (dentine) | 0.00 | 2.67 | 4.77 | 2.91 | 0.41 | 3.43 |
p-tissue 2 | - | - | 4.34 | - | - | - |
Combined US-ESR age (ka) | 121 + 21 -15 | 195 + 34 -23 | 206 + 34 -28 | 223 + 33 -24 | 228 + 65 -40 | 184 +24 -18 |
Combined CSUS-ESR age (ka) | 134 ± 15 | 197 ± 27 | 227 ± 34 | 252 ± 34 | 351 ± 52 | 219 ± 29 |